MS Report from Instrument: LCMS-02 File ..0808 2017-08-08 08-43-26\\BIZ2017-808-WYQ2.D Tgt Mass (CHM): Injection Date : 8 Aug 17 11:26 am +0800 Seq. Line : 33 Sample Name : BIZ2017-808-WYQ2 Location : P1-D-02 Acq. Operator : GHS_886 Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul Acq. Method : D:\\chem32\\1\\DATA\\20170808\\20170808 2017-08-08 08-43-26\\1-POS-3MIN.M Analysis Method : D:\\CHEM32\\1\\DATA\\20170808\\20170808 2017-08-08 08-43-26\\1-POS-3MIN.M Catalog No : HY-13803 Batch#25780 ARP-186 Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C DAD1 B, Sig=214,4 Ref=off 100050000.5 DAD1 C, Sig=254,4 Ref=off mAU60040020000.51 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 7030000200001000000.51 Ion 1, MSD1 1,Target Mass 0 +H Positive, EIC=0.7:1.7 0.050-0.05-0.10.5 Integration Results for DAD1 B, Sig=214,4 Ref=off11.522.5min1.522.5min1.24211.2131.2131.271mAU1.522.5min1.2691.3081.3961.522.5min RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.21 0.02 1201.94 1245.13 99.57 287 1.27 0.02 5.24 5.51 0.43 287 Integration Results for DAD1 C, Sig=254,4 Ref=off RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.21 0.02 893.87 930.47 98.67 287 1.27 0.02 7.03 6.59 0.78 287 1.31 0.02 2.66 2.44 0.29 ND 1.40 0.02 2.38 2.46 0.26 308 Integration Results for MSD1 TIC, MS File RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.24 0.03 81749.35 36667.79 73.57 287 1.35 0.03 29367.86 14846.96 26.43 308LCMS-02 8/9/2017 9:24:31 GHS_8861.351Page 1 of 2
MS Report from Instrument: LCMS-02Ret. Time: 1.24 <<<< POSITIVE SPECTRA >>>> ES-API Positive70006000500040003000 245.1 574.3 595.3200010000200 ES-API Positive4000350030002500200010005000200300400500600700800900m/z 309.31500 282.0 308.2300400500600700800900m/z 287.2Ret. Time: 1.35 LCMS-02 8/9/2017 9:24:31 GHS_886Page 2 of 2
