Data File D:\\AGLIENT 1260\\DATA\\20150901\\20150901 2015-09-01 08-57-32\\BIZ2015-901-DJL6.DSample Name: BIZ2015-901-DJL6=====================================================================Acq. Operator : Li Shan(LCMS-02) Seq. Line : 16Acq. Instrument : HY-LCMS-02 Location : P1-D-08Injection Date : 9/1/2015 10:20:26 AM Inj : 1 Inj Volume : 3.000 µlAcq. Method : D:\\AGLIENT 1260\\DATA\\20150901\\20150901 2015-09-01 08-57-32\\100-1000MS+3MIN- 1.5_(0.02%FA).MLast changed : 9/1/2015 8:57:32 AM by Li Shan(LCMS-02)Analysis Method : D:\\AGLIENT 1260\\DATA\\20150826\\20150826 2015-08-26 09-07-31\\100-1000MS+3MIN- 1.5_(0.02%FA).M (Sequence Method)Last changed : 9/1/2015 2:05:48 PM by Li Shan(LCMS-02) (modified after loading)Method Info : Postive,MS:100-1000,Column ID:A-RP-132,40℃ Catalog No : HY-15559A Batch#17756 A-RP-134 Additional Info : Peak(s) manually integrated DAD1 B, Sig=214,4 Ref=off (D:\\AGLIENT...60\\DATA\\20150901\\20150901 2015-09-01 08-57-32\\BIZ2015-901-DJL6.D) 1.612mAU700600500400300 2.654 2.76910000.511.522.5 3.1342003min ===================================================================== Area Percent Report ===================================================================== Sorted By : SignalMultiplier : 1.0000Dilution : 1.0000Do not use Multiplier & Dilution Factor with ISTDs Signal 1: DAD1 B, Sig=214,4 Ref=off Peak RetTime Type Width Area Height Area # [min] [min] [mAU*s] [mAU] %----|-------|----|-------|----------|----------|--------| 1 1.612 MM 0.0627 2997.66406 796.28180 99.7853 2 2.654 MM 0.0551 3.10647 9.39614e-1 0.1034 3 2.769 MM 0.0467 2.02481 7.22471e-1 0.0674 4 3.134 MM 0.0607 1.31844 3.61970e-1 0.0439 Totals : 3004.11378 798.30585 ===================================================================== *** End of Report ***HY-LCMS-02 9/1/2015 2:05:49 PM Li Shan(LCMS-02)Page 1 of 1
Data File D:\\AGLIENT 1260\\DATA\\20150901\\20150901 2015-09-01 08-57-32\\BIZ2015-901-DJL6.DSample Name: BIZ2015-901-DJL6=====================================================================Acq. Operator : Li Shan(LCMS-02) Seq. Line : 16Acq. Instrument : HY-LCMS-02 Location : P1-D-08Injection Date : 9/1/2015 10:20:26 AM Inj : 1 Inj Volume : 3.000 µlAcq. Method : D:\\AGLIENT 1260\\DATA\\20150901\\20150901 2015-09-01 08-57-32\\100-1000MS+3MIN- 1.5_(0.02%FA).MLast changed : 9/1/2015 8:57:32 AM by Li Shan(LCMS-02)Analysis Method : D:\\AGLIENT 1260\\DATA\\20150826\\20150826 2015-08-26 09-07-31\\100-1000MS+3MIN- 1.5_(0.02%FA).M (Sequence Method)Last changed : 9/1/2015 2:06:49 PM by Li Shan(LCMS-02) (modified after loading)Method Info : Postive,MS:100-1000,Column ID:A-RP-132,40℃ Catalog No : HY-15559A Batch#17756 A-RP-134 Additional Info : Peak(s) manually integrated MSD1 TIC, MS File (D:\\AGLIENT 1260\\DATA\\20150901\\20150901 2015-09-01 08-57-32\\BIZ2015-901-DJL6.D) ES-API, Pos, Sca 1.6161200000100000080000060000040000020000000.511.522.53min HY-LCMS-02 9/1/2015 2:06:50 PM Li Shan(LCMS-02)Page 1 of 2
Data File D:\\AGLIENT 1260\\DATA\\20150901\\20150901 2015-09-01 08-57-32\\BIZ2015-901-DJL6.DSample Name: BIZ2015-901-DJL6MS Signal: MSD1 TIC, MS File, ES-API, Pos, Scan, Frag: 50 Spectra averaged over upper half of peaks. Noise Cutoff: 1000 counts. Reportable Ion Abundance: > 10%. Retention Mol. WeightTime (MS) MS Area or Ion 1.616 8866432 454.20 I 453.20 I 227.10 I 151.80 I*MSD1 SPC, time=1.580:1.653 of D:\\AGLIENT 1260\\DATA\\20150901\\20150901 2015-09-01 08-57-32\\BIZ2015-901-DJL6.D ES-API, 151.8100806040200100200300400500600700800900m/z 227.1Max: 378074 *** End of Report ***HY-LCMS-02 9/1/2015 2:06:50 PM Li Shan(LCMS-02) 454.2 453.2Page 2 of 2