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_R_-_-_-Rolipram_LCMS_13368_MedChemExpress

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Data File D:\\CHEM32\\1\\DATA\\20170515\\20170515 2017-05-15 09-34-01\\CPK2017-515-13368.DSample Name: CPK2017-515-13368=====================================================================Acq. Operator : CLJ_701 Seq. Line : 10Acq. Instrument : LCMS-02 Location : P2-D-02Injection Date : 5/15/2017 10:14:12 Inj : 1 Inj Volume : 1.000 µlAcq. Method : D:\\CHEM32\\1\\DATA\\20170515\\20170515 2017-05-15 09-34-01\\1-POS-3MIN.MLast changed : 5/15/2017 9:34:01 by CLJ_701Analysis Method : D:\\CHEM32\\1\\METHODS\\1-POS-3MIN.MLast changed : 5/15/2017 10:57:52 by CLJ_701 (modified after loading)Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C Catalog No : HY-16900A Batch#13368 A-RP-186 Additional Info : Peak(s) manually integrated*DAD1 B, Sig=214,4 Ref=off (D:\\CHEM32\\1\\DATA\\20170515\\20170515 2017-05-15 09-34-01\\CPK2017-515-13368.D) 1.795 11..661330mAU100080060040020000.511.522.5*DAD1 C, Sig=2,4 Ref=off (D:\\CHEM32\\1\\DATA\\20170515\\20170515 2017-05-15 09-34-01\\CPK2017-515-13368.D) 1.795mAU403020 2.2071000.511.52 2.5153min*2.53min* ===================================================================== Area Percent Report ===================================================================== Sorted By : SignalMultiplier : 1.0000Dilution : 1.0000Do not use Multiplier & Dilution Factor with ISTDs Signal 1: DAD1 B, Sig=214,4 Ref=off Signal has been modified after loading from rawdata file! Peak RetTime Type Width Area Height Area # [min] [min] [mAU*s] [mAU] %----|-------|----|-------|----------|----------|--------| 1 1.613 MF 0.0161 1.295 1.34342 0.0970 2 1.630 FM 0.0144 7.09049e-1 8.18315e-1 0.0531 3 1.795 MM 0.0191 1334.05261 1165.75317 99.8500 Totals : 1336.05720 1167.91491LCMS-02 5/15/2017 10:57: CLJ_701Page

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Data File D:\\CHEM32\\1\\DATA\\20170515\\20170515 2017-05-15 09-34-01\\CPK2017-515-13368.DSample Name: CPK2017-515-13368 Signal 2: DAD1 C, Sig=2,4 Ref=off Signal has been modified after loading from rawdata file! Peak RetTime Type Width Area Height Area # [min] [min] [mAU*s] [mAU] %----|-------|----|-------|----------|----------|--------| 1 1.795 MM R 0.0205 52.37060 47.24986 96.9214 2 2.207 MM R 0.0181 1.10763 1.08433 2.0499 3 2.515 MM R 0.01 5.55874e-1 2.67055e-2 1.0287 Totals : .03411 48.36090 ===================================================================== *** End of Report ***LCMS-02 5/15/2017 10:57: CLJ_701Page 2 of 2

Data File D:\\CHEM32\\1\\DATA\\20170515\\20170515 2017-05-15 09-34-01\\CPK2017-515-13368.DSample Name: CPK2017-515-13368MS Signal: MSD1 TIC, MS File, ES-API, Pos, Scan, Frag: 70 Spectra averaged over upper half of peaks. Noise Cutoff: 1000 counts. Reportable Ion Abundance: > 10%. Retention Mol. WeightTime (MS) MS Area or Ion 1.857 347365 277.15 I 276.15 I*MSD1 SPC, time=1.822:1.888 of D:\\CHEM32\\1\\DATA\\20170515\\20170515 2017-05-15 09-34-01\\CPK2017-515-13368.D ES-API, Po 276.1100806040200100200300400500600700800900m/z 277.1Max: 43240 *** End of Report ***LCMS-02 5/15/2017 10:58:41 CLJ_701Page 2 of 2

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