MS Report from Instrument: HY-LCMS-02 File D:\\CHEM32\\1\\DATA\\BIZ\\BIZ2016-902-WJ3.D Tgt Mass (EZX): 298.00 Injection Date : 2 Sep 16 9:36 am +0800 Seq. Line : 0 Sample Name : BIZ2016-902-WJ3 Location : P1-B-01 Acq. Operator : KFF(LCMS-02) Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul Acq. Method : D:\\Chem32\\1\\METHODS\\1-POS-3MIN.M Analysis Method : D:\\CHEM32\\1\\METHODS\\1-POS-3MIN-PROSRSS.M Catalog No : HY-100512 Batch#21590 Easy-Access Method: '1-POS-3MIN' 298.00 Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C *DAD1 B, Sig=214,4 Ref=off mAU10000.83450000.5*DAD1 C, Sig=254,4 Ref=off mAU30020010000.6750.9111.0670.67511.522.5min*0.8921.0680.51 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 700.67130000200001000001.522.5min*0.511.5 Ion 299, MSD1 299,Target Mass 298 +H Positive, EIC=298.7:299.7 22.5min1501005000.5 Integration Results for DAD1 B, Sig=214,4 Ref=off11.522.5min RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 0.67 0.04 4114.67 1750.88 99.57 263 0.83 0.03 3.25 0.61 0.08 ND 0.91 0.03 4.38 2.18 0.11 ND 1.07 0.04 10.11 4.63 0.24 ND Integration Results for DAD1 C, Sig=254,4 Ref=off RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 0.67 0.04 1071.44 462.33 99.59 263 0.89 0.04 1.31 0.23 0.12 ND 1.07 0.04 3.06 1.34 0.28 NDHY-LCMS-02 9/2/2016 10:58:21 KFF(LCMS-02)Page 1 of 2
MS Report from Instrument: HY-LCMS-02
Ret. Time: 0.67 <<<< POSITIVE SPECTRA >>>> ES-API Positive140012001000800600 196.9 121.0 234.94002000200300400500600700800900m/z 281.1 316.0 263.0 281.0HY-LCMS-02 9/2/2016 10:58:21 KFF(LCMS-02)
620.2 619.0 263.8 282.0 316.2 352.1 337.0Page 2 of 2